Methods in Lignin Chemistry

Methods in Lignin Chemistry edited by Stephen Y. Lin, Carlton W. Dence.

The structural complexity of lignin has continually challenged the in­ genuity of researchers to develop suitable methods for its charac­ terization prior to and following a wide variety of chemical, biologi­ cal, and physical treatments. Initially, activity along these lines was fueled by a desire...

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Bibliographic Details
Corporate Author: SpringerLink (Online service)
Other Authors: Lin, Stephen Y. (Editor), Dence, Carlton W. (Editor)
Format: eBook
Language:English
Published: Berlin, Heidelberg : Springer Berlin Heidelberg : Imprint: Springer, 1992.
Edition:1st ed. 1992.
Series:Springer Series in Wood Science,
Springer eBook Collection.
Subjects:
Agriculture.
Forestry.
Analytical chemistry.
Organic chemistry.
Polymers  .
Materials science.
Electronic resources (E-books)
Online Access:Click to view e-book
Holy Cross Note:Loaded electronically.
Electronic access restricted to members of the Holy Cross Community.
Table of Contents:
  • 1 Introduction
  • 1 Introduction
  • 2 Detection and Determination
  • 2.1 The Detection of Lignin
  • 2.2 The Determination of Lignin
  • 3 Isolation and Purification
  • 3.1 Wood
  • 3.2 Isolation of Lignin from Pulp
  • 3.3 Commercial Spent Pulping Liquors
  • 4 Characterization in Solid State
  • 4.1 Fourier Transform Infrared Spectroscopy
  • 4.2 Ultraviolet Microscopy
  • 4.3 Interference Microscopy
  • 4.4 Electron Microscopy
  • 4.5 Cross Polarization/Magic Angle Spinning Nuclear Magnetic Resonance (CP/MAS NMR) Spectroscopy
  • 4.6 Raman Spectroscopy
  • 4.7 Pyrolysis-Gas Chromatography-Mass Spectrometry
  • 4.8 Thermal Analysis
  • 5 Characterization in Solution: Spectroscopic Methods
  • 5.1 Ultraviolet Spectrophotometry
  • 5.2 Fourier Transform Infrared Spectroscopy
  • 5.3 Proton (1H) NMR Spectroscopy
  • 5.4 Carbon-13 Nuclear Magnetic Resonance Spectrometry
  • 5.5 Electron Spin Resonance (ESR) Spectroscopy
  • 6 Characterization in Solution: Chemical Degradation Methods
  • 6.1 Acidolysis
  • 6.2 Nitrobenzene and Cupric Oxide Oxidations
  • 6.3 Chemical Degradation Methods: Permanganate Oxidation
  • 6.4 Thioacidolysis
  • 6.5 Hydrogenolysis
  • 6.6 Nucleus Exchange Reaction
  • 6.7 Ozonation
  • 7 Functional Group Analysis
  • 7.1 Determination of Total and Aliphatic Hydroxyl Groups
  • 7.2 Determination of Phenolic Hydroxyl Groups
  • 7.3 Determination of Ethylenic Groups
  • 7.4 Determination of Carbonyl Groups
  • 7.5 Determination of Carboxyl Groups
  • 7.6 Determination of Methoxyl Groups
  • 7.7 Determination of Sulfonate Groups and Total Sulfur
  • 8 Determination of Molecular Weight, Size, and Distribution
  • 8.1 Gel Permeation Chromatography
  • 8.2 Light Scattering
  • 8.3 Vapor Pressure Osmometry
  • 8.4 Ultrafiltration
  • 9 Separation of Identification of Low-Molecular Weight Fragments and Model Compounds
  • 9.1 Gas Chromatography-Mass Spectrometry (GC-MS)
  • 9.2 High Performance Liquid Chromatography (HPLC).

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