Chromatography : Principles and Instrumentation.

Chromatography : Principles and Instrumentation.

Provides students and practitioners with a solid grounding in the theory of chromatography, important considerations in its application, and modern instrumentation.-Highlights the primary variables that practitioners can manipulate, and how those variables influence chromatographic separations -Incl...

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Bibliographic Details
Main Author: Vitha, Mark F.
Format: eBook
Language:English
Published: Newark : Wiley, 2016.
Series:Chemical Analysis: A Series of Monographs on Analytical Chemistry and Its Applications
Subjects:
Chromatographic analysis.
Gas chromatography.
Liquid chromatography.
chromatography.
gas chromatography.
liquid chromatography.
SCIENCE > Chemistry > Analytic.
Chromatographic analysis
Gas chromatography
Liquid chromatography
Electronic books.
Online Access:Click for online access
Table of Contents:
  • Cover; Title Page; Copyright; Contents; Preface; Chapter 1 Fundamentals of Chromatography; 1.1 Theory; 1.1.1 Component Separation; 1.1.2 Retention Factor; 1.1.3 Separation; 1.1.4 Resolution and Theoretical Plates; 1.2 Band Broadening; 1.2.1 Diffusion; 1.2.2 Linear Velocity; 1.2.3 Broadening in Open Tubes with No Stationary Phase and No Retention; 1.2.4 Broadening in Open Tubes with a Stationary Phase; 1.2.5 Broadening in a Packed Column; 1.2.6 Putting It All Together; 1.2.7 Practical Consequences of Broadening Theory; 1.3 General Resolution Equation; 1.4 Peak Symmetry.
  • 1.5 Key Operating Variables1.6 Instrumentation; 1.7 Practice of The Technique; 1.7.1 Quantitation; 1.7.2 Internal Standards and the Method of Standard Additions; 1.8 Emerging Trends and Applications; 1.9 Summary; Problems; References; Further Reading; Chapter 2 Gas Chromatography; 2.1 Theory of Gas Chromatographic Separations; 2.1.1 GC Columns and Partitioning; 2.2 Key Operating Variables that Control Retention; 2.2.1 Adjusting Retention Time: Temperature; 2.2.2 Adjusting Retention Time: Temperature Programming; 2.2.3 Adjusting Retention Time: Mobile Phase Flow Rate.
  • 2.2.4 Adjusting Retention Time: The Column and the Stationary Phase2.2.5 Adjusting Retention Time: Summary; 2.2.6 Measures of Retention; 2.3 Gas Chromatography Instrumentation; 2.3.1 Carrier Gas Supply; 2.3.2 The Injection Port and the Solute Injection Process; 2.3.3 Oven/Column Compartment; 2.3.4 Detectors; 2.4 A More Detailed Look at Stationary Phase Chemistry: Kovats Indices and Mcreynolds Constants; 2.4.1 Kovats Retention Indices; 2.4.2 Stationary Phase Selection; 2.5 Gas Chromatography in Practice; 2.5.1 Syringe Washing; 2.5.2 Controls and Blanks/Ghost Peaks; 2.5.3 Autosamplers.
  • 2.5.4 GC Septa2.5.5 Qualitative Analysis; 2.5.6 Quantitative Analysis; 2.5.7 Derivatization; 2.5.8 High-Speed GC; 2.5.9 Tandem GC; 2.5.10 Microfabricated GC; 2.6 A ""Real-World"" Application of Gas Chromatography; 2.6.1 GC and International Oil Trading; 2.7 Summary; Problems; References; Further Reading; Chapter 3 Liquid Chromatography; 3.1 Examples of Liquid Chromatography Analyses; 3.2 Scope of Liquid Chromatography; 3.3 History of LC; 3.3.1 Modern Packing Materials; 3.4 Modes of Liquid Chromatography; 3.4.1 Normal Phase Liquid Chromatography (NPLC).
  • 3.4.2 Reversed-Phase Liquid Chromatography (RPLC)3.4.3 Ion-Exchange Chromatography (IEX); 3.4.4 Hydrophilic Interaction Chromatography (HILIC); 3.4.5 Size Exclusion Chromatography (SEC); 3.4.6 Affinity Chromatography; 3.5 HPLC Instrumentation; 3.5.1 The Proportioning Valve; 3.5.2 Mixing Chamber; 3.5.3 Pumps; 3.5.4 Injection; 3.5.5 The Column and Particles; 3.5.6 Guard Columns; 3.5.7 Detectors; 3.6 Specific Uses of and Advances in Liquid Chromatography; 3.6.1 Chiral Separations; 3.6.2 Preparative-Scale Chromatography.

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