Liquid Chromatography : Fundamentals and Instrumentation.

Annotation

Saved in:
Bibliographic Details
Main Author: Fanali, Salvatore
Other Authors: Haddad, Paul R., Poole, Colin, Riekkola, Marja-Liisa
Format: eBook
Language:English
Published: Saint Louis : Elsevier Science, 2017.
Edition:2nd ed.
Series:Handbooks in Separation Science.
Subjects:
Online Access:Click for online access

MARC

LEADER 00000cam a2200000 i 4500
001 ocn992573108
003 OCoLC
005 20241006213017.0
006 m o d
007 cr |n|---|||||
008 170701s2017 mou o 000 0 eng d
040 |a EBLCP  |b eng  |e pn  |c EBLCP  |d OCLCQ  |d WYU  |d OCLCQ  |d LOA  |d OCLCO  |d OCLCF  |d OCLCO  |d K6U  |d OCLCQ  |d OCLCO  |d OCLCL  |d OCLCQ  |d SXB 
020 |a 9780128093450 
020 |a 0128093455 
035 |a (OCoLC)992573108 
050 4 |a QD79.C454 
049 |a HCDD 
100 1 |a Fanali, Salvatore. 
245 1 0 |a Liquid Chromatography :  |b Fundamentals and Instrumentation. 
250 |a 2nd ed. 
260 |a Saint Louis :  |b Elsevier Science,  |c 2017. 
300 |a 1 online resource (810 pages) 
336 |a text  |b txt  |2 rdacontent 
337 |a computer  |b c  |2 rdamedia 
338 |a online resource  |b cr  |2 rdacarrier 
490 1 |a Handbooks in Separation Science 
588 0 |a Print version record. 
505 0 |a Front Cover; Liquid Chromatography: Fundamentals and Instrumentation; Copyright; Contents; Contributors; Chapter 1: Milestones in the development of liquid chromatography; 1.1 Introduction; 1.1.1 Developments Before 1960; 1.1.2 HPLC at the Beginning; 1.2 HPLC Theory and Practice; 1.2.1 New HPLC Modes and Techniques; 1.2.2 Selection of Conditions for the Control of Selectivity; 1.3 Columns; 1.3.1 Particles and Column Packing; 1.3.2 Stationary Phases and Selectivity; 1.4 Equipment; 1.5 Detectors; Apologies and Acknowledgments; References; Further Reading. 
505 8 |a Chapter 2: Kinetic theories of liquid chromatography2.1 Introduction; 2.2 Macroscopic Kinetic Theories; 2.2.1 Lumped Kinetic Model; 2.2.1.1 van Deemter plate height equation; 2.2.2 General Rate Model; 2.2.2.1 General rate model for monolith columns; 2.2.2.2 General rate model for core-shell particles; 2.2.2.3 Moment analysis; 2.2.3 Lumped Pore Diffusion Model; 2.2.4 Equivalence of the Macroscopic Kinetic Models; 2.2.5 Kinetic Theory of Nonlinear Chromatography; 2.3 Microscopic Kinetic Theories; 2.3.1 Stochastic Model; 2.3.1.1 Stochastic-dispersive model; First passage time. 
505 8 |a 2.3.2 Giddings Plate Height Equation2.3.3 Monte Carlo Simulations of Nonlinear Chromatography; 2.4 Comparison of the Microscopic and the Macroscopic Kinetic Models; References; Further Reading; Chapter 3: Column technology in liquid chromatography; 3.1 Introduction; 3.2 Column Design and Hardware; 3.2.1 Column History in Brief; 3.2.2 Column Hardware; 3.2.3 Column Miniaturization; 3.3 Column Packing Materials and Stationary Phases; 3.3.1 Terminology; 3.3.2 Classification of LC Columns; 3.3.3 Packing Materials [21]; 3.3.3.1 Particle shape, size, and size distribution. 
505 8 |a 3.3.3.2 Pore structure parameters3.3.3.3 Surface functionalization of silica-the key to gaining selectivity; 3.3.3.4 Surface functionalization of silica-the way to bonded silica columns; 3.3.4 Major Synthesis Routes; 3.3.4.1 Physicochemical characterization of bonded silica; 3.3.4.2 Column packing procedures for analytical columns; 3.3.4.3 Examples for selective bonded silica columns; 3.3.4.4 The potential of multimodal or multifunctional bonded columns; 3.4 Column Systems and Operations; 3.4.1 Choice of Average Particle Size and Column Internal Diameter; 3.4.2 Equilibration Time. 
505 8 |a 3.4.3 Choice of Optimum-Flow Conditions3.4.4 Column Back Pressure; 3.4.5 Choice of Column Temperature; 3.4.6 Column Capacity and Loadability; 3.5 Chromatographic Column Testing and Evaluation; 3.5.1 Chromatographic Testing; 3.5.1.1 Hydrophobicity; 3.5.1.2 Silanophilic activity; 3.5.1.3 Polar selectivity; 3.5.1.4 Shape selectivity; 3.5.1.5 Metal content; 3.6 Column Maintenance and Troubleshooting; 3.6.1 Silica-Based Columns; 3.6.1.1 General guidelines; 3.6.2 pH Stability; 3.6.3 Mechanical Stability; 3.6.4 Mobile Phases (Eluents); 3.6.4.1 Proper storage of HPLC columns. 
500 |a 3.6.4.2 Regeneration of a column. 
520 8 |a Annotation  |b Liquid Chromatography: Fundamentals and Instrumentation, Second Edition, is a single source of authoritative information on all aspects of the practice of modern liquid chromatography. It gives those working in both academia and industry the opportunity to learn, refresh, and deepen their understanding of new fundamentals and instrumentation techniques in the field. In the years since the first edition was published, thousands of papers have been released on new achievements in liquid chromatography, including the development of new stationary phases, improvement of instrumentation, development of theory, and new applications in biomedicine, metabolomics, proteomics, foodomics, pharmaceuticals, and more. This second edition addresses these new developments with updated chapters from the most expert researchers in the field. Emphasizes the integration of chromatographic methods and sample preparationExplains how liquid chromatography is used in different industrial sectorsCovers the most interesting and valuable applications in different fields, e.g., proteomic, metabolomics, foodomics, pollutants and contaminants, and drug analysis (forensic, toxicological, pharmaceutical, biomedical)Includes references and tables with commonly used data to facilitate research, practical work, comparison of results, and decision-making. 
650 0 |a Liquid chromatography. 
650 7 |a liquid chromatography.  |2 aat 
650 7 |a Liquid chromatography  |2 fast 
700 1 |a Haddad, Paul R. 
700 1 |a Poole, Colin. 
700 1 |a Riekkola, Marja-Liisa. 
758 |i has work:  |a Liquid chromatography Volume 1 Fundamentals and instrumentation (Text)  |1 https://id.oclc.org/worldcat/entity/E39PCGfFqjRRW47KhX4YDxqB8C  |4 https://id.oclc.org/worldcat/ontology/hasWork 
776 0 8 |i Print version:  |a Fanali, Salvatore.  |t Liquid Chromatography : Fundamentals and Instrumentation.  |d Saint Louis : Elsevier Science, ©2017  |z 9780128053935 
830 0 |a Handbooks in Separation Science. 
856 4 0 |u https://ebookcentral.proquest.com/lib/holycrosscollege-ebooks/detail.action?docID=4884392  |y Click for online access 
903 |a EBC-AC 
994 |a 92  |b HCD